the mother liquors produce further 16 %. After being washed with cold ethanol and ether, the crystals are analytically pure. The proton magnetic resonance spectrum 141 gave the following data (numbers indicate p.p.m with tetramethylsilane as standard) : Si(CH& Si-CHz-Si S-CHI-C C-CH2-0 0.6 3.0 3.8 4
A New Application of the Mitsunobu Reaction in the Synthesis of Phosphonium Salts.
β Scribed by Roman Mazurkiewicz; Tadeusz Gorewoda; Anna Kuznik; Miroslawa Grymel
- Publisher
- John Wiley and Sons
- Year
- 2006
- Weight
- 17 KB
- Volume
- 37
- Category
- Article
- ISSN
- 0931-7597
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π SIMILAR VOLUMES
The Mitsunobu reaction Β± the nucleophilic substitution of an alcoholic hydroxyl group mediated by the redox system trialkylphosphine/dialkyl azodicarobxylate Β± is widely used in the chemistry of biologically active compounds. The paper deals with applications of the Mitsunobu reaction in amino acid
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