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A multinuclear solid state NMR study of the sol–gel formation of amorphous Nb2O5–SiO2 materials

✍ Scribed by K.O. Drake; D. Carta; L.J. Skipper; F.E. Sowrey; R.J. Newport; M.E. Smith

Book ID
108275586
Publisher
Elsevier Science
Year
2005
Tongue
English
Weight
365 KB
Volume
27
Category
Article
ISSN
0926-2040

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Hybrid materials incorporating poly(ethylene glycol) (PEG) with tetraethoxysilane (TEOS) via a sol-gel process were studied for a wide range of compositions of PEG by DSC and high resolution solid-state 13 C-and 29 Si-NMR spectroscopy. The results indicate that the microstructure of the hybrid mater