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A mixed complex of sodium and cobalt(III) with sym-dibenzo-16-crown-5-oxyacetate, [(NH3)5Co(C21H23O3)Na](ClO4)3·2H2O

✍ Scribed by Chyi-Woei Young; Richard A. Bartsch; Robert A. Holwerda

Publisher
Elsevier Science
Year
1982
Tongue
English
Weight
353 KB
Volume
65
Category
Article
ISSN
0020-1693

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✍ Gerhard E. Herberich; Tushar S. Basu Baul; Ulli Englert 📂 Article 📅 2002 🏛 John Wiley and Sons 🌐 English ⚖ 294 KB 👁 2 views

The yellow-orange boratabenzene complex Cb\*Co(3,5-Me 2 C 5 H 3 BNMe 2 ) (1) (Cb\* = C 4 Me 4 ) was readily obtained from [Cb\*Co(NCMe) 3 ]PF 6 and Li(TMEDA)(3,5-Me 2 C 5 H 3 BNMe 2 ). Methanolysis of 1 afforded Cb\*Co(3,5-Me 2 C 5 H 3 BOMe) (2). Complex 2 reacted with MeLi and with BCl 3 to give th