Nanocrystalline CdSe semiconductor was synthesized through a novel solvothermal process, in which CdCl 2 , Se, and Na reacted at 1203C for 6 h in an autoclave, and ethylenediamine was used as a solvent. An XRD pattern indicated a hexagonal CdSe phase. TEM imaging showed that the product consisted of
A Mild Solvothermal Route to Nanocrystalline Titanium Diboride.
β Scribed by Yunle Gu; Yitai Qian; Luyang Chen; Fu Zhou
- Publisher
- John Wiley and Sons
- Year
- 2003
- Weight
- 57 KB
- Volume
- 34
- Category
- Article
- ISSN
- 0931-7597
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Nanocrystalline Cu 7 Te 4 was directly synthesized by the reaction of CuCl 2 ' 2H 2 O and tellurium in an autoclave with ethylenediamine as solvent at 1603C for 10 h. X-ray powder di4raction patterns, X-ray photoelectron spectra, and transmission electron microscope images show that the products are
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were successfully prepared through a simple solvothermal process based on the direct reactions of metal halides with yellow phosphorus at rather mild temperatures (80+1403C) with ethylenediamine used as the solvent. XRD, XPS, and TEM were used to study the phases, compositions, and morphologies of t