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A mild procedure for cleavage of 1,6-anhydro sugars

โœ Scribed by Zottola, Mark; Rao, B. Venkateswara; Fraser-Reid, Bert

Book ID
119958322
Publisher
The Royal Society of Chemistry
Year
1991
Tongue
English
Weight
207 KB
Volume
14
Category
Article
ISSN
0022-4936

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Ferric chloride: a mild and versatile re
Ferric chloride: a mild and versatile reagent for the formation of 1,6-anhydro glucopyranoses
โœ Pedro O Miranda; Ignacio Brouard; Juan I Padrรณn; Jaime Bermejo ๐Ÿ“‚ Article ๐Ÿ“… 2003 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 322 KB

A novel method for the preparation of 1,6-anhydro glucopyranoses (mono-and disaccharides) utilizing anhydrous FeCl 3 as Lewis acid is described. Treatment of methyl 6-O-benzyl and 6-O-p-methoxybenzyl-a/b D-glucopyranosides derivatives with FeCl 3 in CH 2 Cl 2 at room temperature and 40ยฐC afforded 1,