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A low-temperature refinement of tris­[N,N′-bis­(2-hydroxy­ethyl)dithio­carbamato-κ2S,S′]anti­mony(III)

✍ Scribed by Tiekink, Edward R. T. ;Young, David J.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
474 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, [Sb(C 5 H 10 NO 2 S 2 ) 3 ], has been redetermined at 93 K, allowing a detailed analysis of the crystal packing, which is dominated by O-HÁ Á ÁO hydrogen bonding. Each terminal hydroxyl group participates in a 12-membered [Á Á ÁO-H] 6 ring, leading to a three-dimensional array. metal-organic papers Acta Cryst. (2006). E62, m1887-m1889 Tiekink and Young [Sb(C 5 H 10 NO 2 S 2 ) 3 ] m1889

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