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A highly stereocontrolled total synthesis of the polyether antibiotic salinomycin. Crucial role of the 40-metoxybenzyl; (mpm) protecting group for hydroxy functions

✍ Scribed by Kiyoshi Horita; Yuji Oikawa; Satoshi Nagato; Osamu Yonemitsu


Publisher
Elsevier Science
Year
1988
Tongue
French
Weight
310 KB
Volume
29
Category
Article
ISSN
0040-4039

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✦ Synopsis


Salinomycin was synthesized from D-glucose, D-mannitol, and ethyl L-lactate via coupling of Cl-C9, ClO-C17, and C18-C30 segments. Benzyl-type protecting groups as well as regioand stereoselective reactions played a crucial role.