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A Highly Active and General Catalyst for the Stille Coupling Reaction of Unreactive Aryl, Heteroaryl, and Vinyl Chlorides under Mild Conditions

✍ Scribed by Lee, Dong-Hwan; Qian, Yingjie; Park, Ji-Hoon; Lee, Jong-Suk; Shim, Sang-Eun; Jin, Myung-Jong

Book ID: 120406069
Publisher: John Wiley and Sons
Year: 2013
Tongue: English
Weight: 314 KB
Volume: 355
Category: Article
ISSN: 1615-4150
DOI: 10.1002/adsc.201300075

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Scheme 1. Synthesis of magnetic nanoparticle-supported (b-oxoiminato)(phosphanyl) palladium complex 4. a) NH 2 (CH 2 ) 3 Si(OEt) 3 , microwave heating; b) EtOTl, [Pd 2 (m-Cl) 2 Me 2 (PPh 3 ) 2 ], tetrahydrofuran, RT; c) tetraethyl orthosilicate; d) 2, toluene, 100 8C, 12 h.