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A general synthesis of optically active phosphines, phosphinites and thiophosphinites from alkylthio(alkylseleno)phosphonium salts and tris(dimethylamino)phosphine as a thiophilic agent

✍ Scribed by J. Omelańczuk; M. Mikołgajczyk


Publisher
Elsevier Science
Year
1984
Tongue
French
Weight
249 KB
Volume
25
Category
Article
ISSN
0040-4039

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✦ Synopsis


Tris(dimethylaminolphosphine was found to be a suitable thiophilic reagent which converts optically active aZkyZthiofaZkyZseZeno!phosphosphonium salts into chiral tertiary phosphines and phosphinites

with a high stereosetectivity. The first synthesis of opticaZZy active thiophosphinites from bislal-kyZthioiphosphonium salts and trisldimethyZaminolphosphine is also reported.