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A general purpose n.m.r. microcell system suitable for volatile, air sensitive and toxic samples

✍ Scribed by Jassim M. A. Al-Rawi; James P. Bloxsidge


Publisher
John Wiley and Sons
Year
1977
Tongue
English
Weight
111 KB
Volume
10
Category
Article
ISSN
0749-1581

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✦ Synopsis


Abstract

A microcell system that is convenient to fill and which can be evacuated and/or filled with gas or vapour has been developed for handling tritiated n.m.r. samples and has subsequently proved to have a more general application. A 3 mm tube, after the removal of a 5 mm filling extension, is sleeved into a 5 mm n.m.r. tube or used directly in a reduced diameter probe.