✦ LIBER ✦
A four factor simplex optimization of a serially coupled open tublar columns gas chromatographic system
✍ Scribed by Bakeas, Evangelos B. ;Siskos, Panayotis A.
- Publisher
- John Wiley and Sons
- Year
- 1996
- Tongue
- English
- Weight
- 571 KB
- Volume
- 19
- Category
- Article
- ISSN
- 0935-6304
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✦ Synopsis
Abstract
Optimization of a gas chromatographic system with two capillary columns coupled in series in a single oven for the linear temperature programmed separation of a mixture of C~1~C~10~ hydrocarbons has been carried out using the simplex optimization method. The following four selectivity parameters were optimized: the initial temperature of the oven; the initial hold time; the temperature programmed rate; and the pressure at the mid‐point of the system. The optimization procedure was monitored by the C~p~ criterion.