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A facile total synthesis of ent-17β-estradiol and structurally related analogues

✍ Scribed by Zu Yun Cai; Douglas F. Covey

Book ID
116892031
Publisher
Elsevier Science
Year
2007
Tongue
English
Weight
535 KB
Volume
72
Category
Article
ISSN
0039-128X

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A facile synthesis of ascamycin and rela
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The nucleoside antibiotic ascamycin [2-chloro-5'-g-[I+(k-alanyljsulfamoyl) adenosine (l)] has been synthesized by an improved procedure involving the direct condensation of 2-chloro-2',3'-~-isopropylidene-5'-~-sulfamoyladenosine (3) with Bock-Ala-O% in DMF and in the presence of DBU. followed by rem