A facile synthesis of cyclic enecarbamates using Dess–Martin periodinane

✍ Scribed by Chengzhi Yu; Longqin Hu

• Book ID: 104231059
• Publisher: Elsevier Science
• Year: 2001
• Tongue: French
• Weight: 92 KB
• Volume: 42
• Category: Article
• ISSN: 0040-4039
• DOI: 10.1016/s0040-4039(01)00998-4

✦ Synopsis

A simple and efficient synthesis of cyclic enecarbamates from v-hydroxycarbamates via tandem oxidative cyclizationdehydration was achieved in 84% to quantitative yield using Dess-Martin periodinane in methylene chloride.