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A facile synthesis of aromatic trifluoromethyl compounds via orthothio esters

✍ Scribed by Donald P. Matthews; Jeffrey P. Whitten; James R. McCarthy

Publisher: Elsevier Science
Year: 1986
Tongue: French
Weight: 185 KB
Volume: 27
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(00)85082-0

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✦ Synopsis

Aromatic trifluoromethyl compounds (2) are prepared by treatment of aromatic orthothio esters (Ll with 1,3-dibromo-5,5_dimethylhydantoin (DBH) or N-bromosuccinimide (NBS) followed by HF/pyridine complex. The starting materials (1) were readily obtained by literature methodology.

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