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A Facile Procedure for Preparation of Carboxylic Sulfonic Anhydrides Under Solvent-Free Conditions

✍ Scribed by Hajipour, A. R.; Mazloumi, Gh.


Book ID
125519793
Publisher
Taylor and Francis Group
Year
2003
Tongue
English
Weight
73 KB
Volume
178
Category
Article
ISSN
1042-6507

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A facile preparation of (2,4,6-14C)-cyan
✍ S. P. Patil; D. Padmanabhan πŸ“‚ Article πŸ“… 2002 πŸ› John Wiley and Sons 🌐 French βš– 63 KB

## Abstract (2,4,6‐^14^C)‐Cyanuric acid was prepared from ^14^C‐urea by the heterocyclization of the latter in the presence of ammonium chloride. This procedure involves solvent‐free fusing of the reactants in a vacuum sealed glass tube. The product was purified by ion‐exchange column chromatograph