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A Convenient Synthesis of Phosphonothioic Acids.

✍ Scribed by Krzysztof Swierczek; John W. Peters; Alvan C. Hengge

Publisher
John Wiley and Sons
Year
2003
Weight
239 KB
Volume
34
Category
Article
ISSN
0931-7597

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✦ Synopsis

Abstract

For Abstract see ChemInform Abstract in Full Text.

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## Abstract Monoamination of dibromopyridines (I) and (VIII) followed by carbonylation and subsequent hydrolysis of methyl esters (VI) and (X) furnish (alkylamino)pyridinecarboxylic acids (VII) and (XI) in satisfactory to good yields, though the 3,5‐dibromopyridine (VIII) reacts more slowly.