𝔖 Bobbio Scriptorium
✦   LIBER   ✦

A convenient synthesis of both the anomers of ethyl (2,3,4,6-tetra-O-benzyl-D-glucopyranosyl)acetate

✍ Scribed by Diego Monti; Paola Gramatica; Giovanna Speranza; Paolo Manitto


Book ID
104227986
Publisher
Elsevier Science
Year
1987
Tongue
French
Weight
171 KB
Volume
28
Category
Article
ISSN
0040-4039

No coin nor oath required. For personal study only.


πŸ“œ SIMILAR VOLUMES


ChemInform Abstract: Convenient Synthesi
✍ W. KUDELSKA πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons βš– 42 KB πŸ‘ 2 views

Convenient Synthesis of S-and Se-(2,3,4,6-Tetra-O-benzyl-Dglucopyranosyl)-phosphorothioate, Phosphoroselenoate and Phosphorodithioate. -BF 3 -mediated reaction of both 1-O-unprotected and 1-O-acyl sugars (I) with phosphorothioate (II), -selenate (IV) or -dithiolate (VI) provides the corresponding g

A Convenient Procedure for he Synthesis
✍ Roland Hoos; Andrew B. Naughton; Andrea Vasella πŸ“‚ Article πŸ“… 1993 πŸ› John Wiley and Sons 🌐 German βš– 445 KB

## Abstract __Swern__ oxidation of 2,3,4,5‐tetra‐__O__‐benzyl‐D‐glucose (1) followed by ammonolysis gave the crystalline amide 3 which was oxidized (DMSO/pyridine Β· SO~3~) to yield the oxo‐amide 4 and the hydroxy‐lactams 5 and 6. Cyclization of 4 to the very slowly equilibrating 5 and 6 was complet