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A Convenient Synthesis and a NMR Study of the Diammoniate of Diborane

✍ Scribed by Dr. Hima K. Lingam; Dr. Xuenian Chen; Prof. Ji-Cheng Zhao; Prof. Sheldon G. Shore

Book ID
112020010
Publisher
John Wiley and Sons
Year
2012
Tongue
English
Weight
201 KB
Volume
18
Category
Article
ISSN
0947-6539

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Rapid chemical syntheses of D-[l-"C] glucopyranose and D-[ l-llC] galactopyranose starting from D-arabinopyranose and D-lyxopyranose, respectively, are described. The use of diborane for reduction of intermediates in highly effective for reducing the time required.