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A Convenient Procedure for the Synthesis of Acetals from α-Halo Ketones

✍ Scribed by Rolf Carlson; Hanna Gautun; Andreas Westerlund

Publisher
John Wiley and Sons
Year
2002
Tongue
English
Weight
76 KB
Volume
344
Category
Article
ISSN
1615-4150

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An efficient and convenient procedure fo
An efficient and convenient procedure for the synthesis of nα-Fmoc-O-monobenzyl phosphonotyrosine
✍ B.K. Handa; C.J. Hobbs 📂 Article 📅 1998 🏛 John Wiley and Sons 🌐 English ⚖ 184 KB

An efficient procedure is described for the synthesis of N h -Fmoc-O-monobenzyl phosphonotyrosine from the corresponding dibenzyl derivative by monodebenzylation in the presence of sodium iodide. A simple work up procedure removes the by-products and the monobenzylated phosphono product is obtained