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A Convenient Procedure for the Preparation of 1-(Diisopropylamino)phospholes − Application to the Synthesis of New 2,2′-Biphosphole Disulfides

✍ Scribed by Jérôme Hydrio; Maryse Gouygou; Frédéric Dallemer; Gilbert G. A. Balavoine; Jean-Claude Daran

Publisher: John Wiley and Sons
Year: 2002
Tongue: English
Weight: 457 KB
Volume: 2002
Category: Article
ISSN: 1434-193X
DOI: 10.1002/1099-0690(200202)2002:4<675::aid-ejoc675>3.0.co;2-z

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✦ Synopsis

A convenient one-pot procedure for the preparation of 1-(diisopropylamino)phospholes has been developed. These phospholes have been used in a multistep procedure for synthesizing two new 2,2Ј-biphosphole disulfide compounds. The structures and stereochemistry of these compounds have been studied by X-ray diffraction analysis and by molecular [a]

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