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A CONVENIENT PREPARATION OF SUBERIC ACID. CONCERNING THE HOMOGENEITY AND USE IN SYNTHESIS OF POLYMETHYLENE CHLOROBROMIDE PREPARATIONS

โœ Scribed by CASON, JAMES; WALLCAVE, LAWRENCE; WHITESIDE, CHARLES N.

Book ID
126029706
Publisher
American Chemical Society
Year
1949
Tongue
English
Weight
588 KB
Volume
14
Category
Article
ISSN
0022-3263

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Methyl 8-oxooctanoate-4,5-d and methyl 12-oxododecanoate-4,5,8,9-d4 were prepared for use as inzermediates in the synthesis of a series of labelled fatty acid methyl esters. Synthesis of the two compounds began with monoozonization and sodium acetate cleavage of 1,4-cyclooctadiene and 1,5,9-~yclodod