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A convenient preparation of functionalized arylzinc compounds by the reaction of zinc/silver-graphite with aryl iodides

✍ Scribed by Alois Fürstner; Robert Singer; Paul Knochel

Publisher
Elsevier Science
Year
1994
Tongue
French
Weight
343 KB
Volume
35
Category
Article
ISSN
0040-4039

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Monoiodoarenes undergo reductive coupling to produce biaryls in high yields in the presence of less than 0.1 mol % of palladacyle and NNdiisopropylethylamine in DMF at 1OO'C. Under similar reaction conditions, pdiiodobenzene produces poly-p-phenylene in greater than 85% isolated yields.