A contribution to the indexing of transmission electron diffraction patterns
β Scribed by Dr. A. Messerschmidt
- Publisher
- John Wiley and Sons
- Year
- 1975
- Tongue
- English
- Weight
- 399 KB
- Volume
- 10
- Category
- Article
- ISSN
- 0232-1300
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β¦ Synopsis
Abstract
A method for the indexing of TED spot patterns is presented. The reduced cell of the TED pattern defined by the two shortest vectors, which enclose an acute angle, serves as reference cell for the indexing. The dβvalues of both the cell defining vectors and of their sum and difference vectors are determined being the four largest dβvalues, which can be determined from the pattern. These four dβvalues are compared with suitable dβvalue sets of the possible crystalline phases and probable phase identifications are made. Generally, there exist several indexing variants for the individual dβvalues of the separate phase identification possibilities. It is possible to find the correct indexing by the determination of the indices of the sum and difference vectors, occasionally, for one pair of the indexing variant from the vectors defining the reference cell and by comparison of these indices with the indexing variants for the dβvalues of the sum and difference vectors of the corresponding phase identification variant. The measuring and calculation of the intervectorial angles formerly necessarily hasn't to be made in this method. However, the determination of the sum and difference vectors involves it. The reliability of the indexing can be increased in a strong manner if two or three different reciprocal lattice planes of the specimen under investigation are recorded in the corresponding TED patterns and if, in the following, these patterns can be indexed by the mentioned method without any doubt.
π SIMILAR VOLUMES
Electron diffraction patterns generated from phases that have low crystallographic symmetry are difficult and tedious to analyze by conventional techniques. This paper describes a computation scheme that can index electron diffraction patterns efficiently and quickly and be easily implemented on a p