Attenuated total reflection-infrared (ATR-IR) spectroscopy and wide-angle x-ray diffraction (WAXD) were used to determine the macromolecular orientation of a series of six uniaxially oriented polypropylene sheets with elongations of 0% to 500%. The orientation functions were expressed as fractions o
A Comparison of Rutherford Backscattering Spectroscopy and X-Ray Diffraction to Determine the Composition of Thick InGaN Epilayers
β Scribed by S. Srinivasan; R. Liu; F. Bertram; F.A. Ponce; S. Tanaka; H. Omiya; Y. Nakagawa
- Publisher
- John Wiley and Sons
- Year
- 2001
- Tongue
- English
- Weight
- 88 KB
- Volume
- 228
- Category
- Article
- ISSN
- 0370-1972
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β¦ Synopsis
In this paper, we report the measurements of indium composition of thick InGaN epilayers by X-ray diffraction (XRD) and Rutherford backscattering spectroscopy (RBS). In order to account for the biaxial stress in the InGaN epilayers, we determined both a and c lattice parameters in a q/2q scan. Indium composition was determined by simultaneous application of Vegard's law to both lattice parameters and by considering the relationship between the lattice parameters under strain. These composition values are compared with values determined by RBS. The value of elastic constants used in these calculations is critical and we show that by careful choice we can obtain a good correlation between the XRD and RBS measurements.
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Previously, it has been shown that the correlation of deuterium quadrupolar tensors by spin diffusion under slow magic-angle-spinning conditions can provide accurate measurements of their relative orientation. In the present work we apply the technique to the cyclo-b-peptide cyclo with its amide hy
## Abstract A comprehensive ^31^P solidβstate NMR study of Ru(Ξ·^1^βPh~2~PCH~2~CH~2~OCH~3~)~2~(Ξ·^2^βen)Cl~2~ (en = ethylenediamine) (1), by 1D (contact time variation, inversionβrecovery, SPARTAN) and 2D techniques (homonuclear __J__βresolved, SECSY) indicated that the crystal structure of 1 should