The relative sensitivities of steam distillation, hot headspace and adsorption wire techniques for fire accelerant recovery were compared under conditions designed to simulate the more extreme casework conditions of tenacious adsorption of accelerant to fire debris. Hot headspace performed least wel
A comparison of extraction and adsorption methods for the recovery of accelerants from arson debris
β Scribed by Luis Frontela; Jose A Pozas; Leandro Picabea
- Publisher
- Elsevier Science
- Year
- 1995
- Tongue
- English
- Weight
- 562 KB
- Volume
- 75
- Category
- Article
- ISSN
- 0379-0738
No coin nor oath required. For personal study only.
β¦ Synopsis
Two different methods of recovering arson accelerants from fire debris are compared: distillation with addition of n-hexane and adsorption onto activated charcoal. Both procedures involve the use of the gas chromatography/mass spectrometry (GC/MS) utilizing specific mass ion programs. Some casework examples have been analyzed and the results show that, in spite of the advantages of short application times in the adsorption method, the distillation technique presented a higher degree of efficiency.
π SIMILAR VOLUMES
Comparison of extraction methods for the recovery, amplification and species-specific analysis of DNA from bone and bone meals We report the effect of several parameters on the efficiency of recovery of DNA from animal bones. The effects of preheating the samples (at either 607C or 1007C) at differe
## Abstract Batch and continuous solvent extraction methods were evaluated, using an alcoholic model system, to select the best alternative for the isolation of volatile aroma compounds from distilled alcoholic beverages. Recoveries using pentane, pentaneβdiethyl ether (2:1) and dichloromethane wer