## Abstract It is shown that highโresolution ^1^H NMR spectra of intact excised tissues and organs can be obtained by rotating the sample slowly about an axis at the magic angle of 54ยฐ44โฒ with the external magnetic field. In this way tissue and cellular damage invoked by standard magic angle spinni
A comparison of cell and tissue extraction techniques using high-resolution 1H-NMR spectroscopy
โ Scribed by J. E. Le Belle; N. G. Harris; S. R. Williams; K. K. Bhakoo
- Publisher
- John Wiley and Sons
- Year
- 2002
- Tongue
- English
- Weight
- 99 KB
- Volume
- 15
- Category
- Article
- ISSN
- 0952-3480
- DOI
- 10.1002/nbm.740
No coin nor oath required. For personal study only.
๐ SIMILAR VOLUMES
## Abstract Highโresolution magic angle spinning (HRMAS) ^1^H NMR spectroscopy is ideal for monitoring the metabolic environment within tissues, particularly when spectra are weighted by physical properties such as __T__~1~ and __T__~2~ relaxation times and apparent diffusion coefficients (ADCs). I
o-Benzenediazonium carboxylates couple with methylene-active compounds to yield hydrazo derivatives with high purity. The 'H and 13C NMR data of eleven such products are presented and analysed. The predominance of the hydrazo over the azo form is consistent with accepted criteria. Furthermore, evide
## Abstract This study explored the utility of ^1^H and ^13^C magnetic resonance spectroscopy to study a neuronโenriched preparation made from rat cerebrum. The preparation contained high concentrations of __N__โacetylaspartate and ฮณโaminobutyric acid and low concentrations of glutamine, indicating
It is demonstrated that a high-resolution (1)H NMR spectrum of excised rat liver can be obtained using the technique of magic angle turning (MAT) at a sample spinning rate of 1 Hz. A variant of the phase-corrected MAT (PHORMAT) pulse sequence that includes a water suppression segment was developed f