A comparative study of the resolving power of both conventional thermogravimetry and constant rate thermal analysis
β Scribed by J.M. Criado; A. Ortega; F.J. Gotor
- Publisher
- Elsevier Science
- Year
- 1992
- Tongue
- English
- Weight
- 263 KB
- Volume
- 203
- Category
- Article
- ISSN
- 0040-6031
No coin nor oath required. For personal study only.
π SIMILAR VOLUMES
## Abstract A convenient synthesis of 4βalkylβ1,3βdiarylpyrazoles (**2**) under microwave irradiation as well as conventional thermal method using Vilsmeier cyclization is reported. Microwave irradiation has resulted in the reduction of time from hours to seconds.
The mechanism of the thermal decomposition of smithsonite has been determined from a comparison of the results obtained from isothermal, linear heating rate (TG), and Constant Rate Thermal Analysis (CRTA) experiments. Two important precautions have been taken in this work. Firstly, the chemical comp