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A class of new silylating reagents. I. A mild method for introduction of the tert-butyldimethylsilyl group.

✍ Scribed by Tank Veysoglu; Lester A. Mitscher

Publisher: Elsevier Science
Year: 1981
Tongue: French
Weight: 241 KB
Volume: 22
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(01)90301-6

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✦ Synopsis

t-Butyldimethylsilyl enol ethers of pentane-2,4-dione and methyl acetoacetate react rapidly at room temperature to give high isolated yields of the t-butyldimethylsilyl ethers of a variety of alcohols.

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