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A chiral oxazolidin-2-one-derived Reissert compound

✍ Scribed by Evain, Michel ;Pauvert, Mickaël ;Collet, Sylvain ;Guingant, André

Book ID
104479720
Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
191 KB
Volume
58
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê R factor = 0.035 wR factor = 0.085 Data-to-parameter ratio = 9.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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Transposition of the dormant methyl group from C-1 in chiral oxazolidin-2-one 2 to C-7 in a six step synthetic sequence from (IR)-camphor 5 creates a novel transfigomer 4 with sufficient n-topological bias to induce excellent levels of asymmetric induction in Lewis-acid catalysed Diels-Alder reactio