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A Chiral and Colorful Redox Switch: Enhanced π Acidity in Action

✍ Scribed by Dr. Jiří Míšek; Andreas Vargas Jentzsch; Dr. Shin-ichiro Sakurai; Daniel Emery; Dr. Jiri Mareda; Prof. Stefan Matile

Publisher: John Wiley and Sons
Year: 2010
Tongue: English
Weight: 574 KB
Volume: 49
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.201003722

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The acetonitrile complex [(η 5 -C 5 H 5 )Re(NO)(NCCH 3 )(CO)] + BF 4 -(1) and P(4-C 6 H 4 CF 3 ) 3 slowly react (2 d, room temperature) to give the substitution product [(η 5 -C 5 H 5 )Re(NO){P(4-C 6 H 4 CF 3 ) 3 }(CO)] + BF 4 -(3, 85%). The reaction of 1 and less nucleophilic P(C 6 F 5 ) 3 must be