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A Broad Substrate-Scope Method for Fast, Efficient and Selective Hydrogen Peroxide-Epoxidation

โœ Scribed by Isaac Garcia-Bosch; Xavi Ribas; Miquel Costas

Book ID
101423054
Publisher
John Wiley and Sons
Year
2009
Tongue
English
Weight
183 KB
Volume
351
Category
Article
ISSN
1615-4150

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โœ Albrecht Berkessel; Marc R.M Andreae ๐Ÿ“‚ Article ๐Ÿ“… 2001 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 55 KB

We have found that the Baeyer-Villiger oxidation of cyclohexanone with hydrogen peroxide in 1,1,1,3,3,3-hexafluoro-2propanol as solvent is catalyzed by Brรธnsted acids: in the presence of 1 mol% of p-TsOH, transformation to o-caprolactone occurs rapidly and under mild conditions. Epoxidation of 1-oct