A 2-propanol solvate of (RS)-phenylsuccinic acid
✍ Scribed by Fischer, Andreas ;Profir, Veronica M.
- Book ID
- 104481951
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 210 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
A solvate of (RS)-phenylsuccinic acid (RS-PSA) has been obtained from 2-propanol (IPA). The compound, C 10 H 10 O 4 ÁC 3 H 8 O, crystallizes in the monoclinic crystal system (space group C2/c). It features molecules of the S form of the acid, one of whose carboxy groups is connected to one carboxy group of a molecule of the opposite chirality via two hydrogen bonds. The second carboxy group of the S molecule is connected to two other S molecules via the OH groups of two 2-propanol solvent molecules.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 173 K Mean '(C±C) = 0.007 A Ê Disorder in solvent or counterion R factor = 0.069 wR factor = 0.225 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The goal of the present work was to understand the effect of relative humidity (RH) and temperature on the molecular structure, crystal structure, and physical properties of warfarin sodium 2-propanol solvate (W). After previous determination of the crystal structure of W, which corresponds to a 1:1
## Abstract Electrochemical dicarboxylation of styrene in the presence of atmospheric pressure of CO~2~ with a Ti cathode and a Mg rod anode readily took place efficiently in an acetonitrile solution containing 0.1 mol·L^−1^ tetraethylammonium bromide to give 2‐phenylsuccinic acid. Influences of th