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8-Methylspiro(syn-10,11-benzo-8-azatricyclo[5.2.2.01,5]undec-10-ene)-9,3'-[3H]naphth[1,2-b][1,4]oxazine

✍ Scribed by Pèpe, G. ;Laréginie, P. ;Samat, A. ;Guglielmetti, R. ;Zaballos, E.


Book ID
114511858
Publisher
International Union of Crystallography
Year
1995
Tongue
English
Weight
303 KB
Volume
51
Category
Article
ISSN
0108-2701

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The title compound, C 25 H 20 N 6 O 3 ÁCHCl 3 , a rigid glycoluril derivative, is an intermediate for the synthesis of molecular tweezers. The crystal structure is stabilized by intermolecular C-HÁ Á ÁO and N-HÁ Á ÁO hydrogen bonds. The chloroform solvent molecule is disordered over two positions; t