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7β-hydroxy bile alcohols: Facile synthesis and 2D 1H NMR studies of 5β-cholestane-3α,7β,12α,25-tetrol

✍ Scribed by B. Dayal; N.H. Ertel; J. Padia; K.R. Rapole; G. Salen

Book ID
117213844
Publisher
Elsevier Science
Year
1997
Tongue
English
Weight
606 KB
Volume
62
Category
Article
ISSN
0039-128X

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Bile alcohol glucuronides: regioselectiv
Bile alcohol glucuronides: regioselective O-glucuronidation of 5β-cholestane-3α,7α,12α,25-tetrol and 24-nor-5β-cholestane-3α,7α,12α,25-tetrol
✍ Bishambar Dayal; Gerald Salen; Janak Padia; Sarah Shefer; George S. Tint; Gino S 📂 Article 📅 1993 🏛 Elsevier Science 🌐 English ⚖ 746 KB

## ABSTRAm A facile and regiocontrolled procedure for the preparation of S~-cholestane-3a,7c,l2~,25-tetrol-3-O-fi-o-glucuronide and its corresponding C-26 analogue is described. The method involves direct coupling of bile alcohols, namely, 5/3-cholestane-3rY,7~,12a,25-tetrol and 24-nor-Sp-cholesta