73Ge: a new high resolution PAC probe
β Scribed by J. G. Correia; H. Haas; J. G. Marques; A. A. Melo; J. C. Soares
- Book ID
- 112373739
- Publisher
- Springer
- Year
- 1993
- Tongue
- English
- Weight
- 363 KB
- Volume
- 80
- Category
- Article
- ISSN
- 0304-3843
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High-resolution solid-state magic angle spinning (73)Ge NMR spectra of some organogermanium compounds were measured. Most tetrasubstituted germanes with identical substituents exhibited signals except for one case. Tetrasubstituted germanes with two kinds of different but somewhat similar substituen
## Abstract Highβresolution solidβstate magic angle spinning ^73^Ge NMR spectra of hexavalent germanium compounds, i.e. diiodogermylene (**1a**) and bis(1βpyrrolyl)(__meso__βtetraphenylporphyrinato)germanium (**3a**), were determined. To the best of our knowledge, this is the first example of highβ