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703. Aza-steroids. Part VI. Beckmann rearrangement of some α-hydroxy-ketoximes

✍ Scribed by Shoppee, C. W. ;Roy, S. K.


Book ID
120837457
Publisher
The Royal Society of Chemistry
Year
1963
Weight
332 KB
Volume
0
Category
Article
ISSN
0368-1769

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Snatzlce and Pehlhaber' reported the isolation, in yields up to 5C$, of an unsaturated diaoetate on treatment of the triacetate (I) with acetic anhydride in the presence of a variety of acidic catalysts at 80' or 440'. Theee authors tentatively assigned structure (II) to the diacetate but later comm