7-(4-Fluorophenyl)-8H-benzo[h]indeno[1,2-b]quinolin-8-one
✍ Scribed by Tu, Shu-Jiang ;Zhang, Yan ;Jia, Run-Hong
- Publisher
- International Union of Crystallography
- Year
- 2006
- Tongue
- English
- Weight
- 119 KB
- Volume
- 62
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
The title compound, C 27 H 24 N 2 O 4 , has been synthesized by the reaction of 4-nitrobenzaldehyde, 3-(cyclopropylamino)-5,5dimethylcyclohex-2-enone and 1,3-indanedione in a mixed solvent of ethylene glycol and acetic acid under microwave irradiation. The dihydropyridine ring adopts a boat conforma
Single-crystal X-ray study T = 298 K Mean (C-C) = 0.008 A Disorder in main residue R factor = 0.066 wR factor = 0.245 Data-to-parameter ratio = 12.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean (C-C) = 0.002 A R factor = 0.025 wR factor = 0.069 Data-to-parameter ratio = 12.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
## Abstract magnified image Treatment of methyl propiolate and 2‐(thiophen‐2‐yl)benzaldehyde, 2‐(thiophen‐3‐yl)benzaldehyde or 2‐(furan‐3‐yl)benzaldehyde with tetrabutylammonium iodide/zirconium (IV) chloride or treatment of methyl acrylate and the same aldehydes with 1,4‐diazabicyclo[2,2,2]octane