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(5α,8α,9β,11S)-5,7,8,9-Tetra­hydro-11-(fluoro­meth­yl)-9-(3,4,5-trimethoxy­phen­yl)-5,8-methano-1,3-dioxolo[4,5-h][2]benzoxepin

✍ Scribed by Zhong, Jian-Hua ;Jian, Shan-Zhong ;He, Xue-Ying ;Wang, Yan-Guang


Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
325 KB
Volume
61
Category
Article
ISSN
1600-5368

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9-(2,6-Dihydroxy­phen­yl)-3,3,6,6-tetra­
✍ Jang, Hong ;Li, Tuanjie ;Tu, Shujiang ;Zou, Xiang 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 97 KB

The title compound, C 30 H 33 NO 4 , was synthesized by the reaction of 2,6-dihydroxybenzaldehyde with p-toluidine and 5,5-dimethylcyclohexane-1,3-dione in glycol under microwave irradition. X-ray analysis reveals that the dihydropyridine ring is in a distorted boat conformation and that the cyclohe