Single-crystal X-ray study T = 170 K Mean '(C±C) = 0.004 A Ê Disorder in main residue R factor = 0.047 wR factor = 0.139 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
5,7,3′-Trihydroxy-6,8-di-C-methyl-4′,5′-dimethoxyflavanone from Alluaudiopsis marnieriana
✍ Scribed by Zafera Rabesa; Bernard Voirin
- Publisher
- Elsevier Science
- Year
- 1983
- Tongue
- English
- Weight
- 212 KB
- Volume
- 22
- Category
- Article
- ISSN
- 0031-9422
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.002 A Ê R factor = 0.038 wR factor = 0.101 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê R factor = 0.068 wR factor = 0.198 Data-to-parameter ratio = 9.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The asymmetric unit of (I), showing 30% probability displacement ellipsoids and the atom-numbering scheme. H atoms have been omitted.
## Abstract A novel synthesis of substituted thieno[3,2‐__c__]azepinones is described. This new approach uses 5,5‐dimethyl‐1,3‐cyclohexanedione (dimedone) as the starting material. Oxime intermediates are obtained in three steps from the aforementioned diketone. Using these intermediates, the title