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5,6-Dioxo-1,10-phenanthrolin-1-ium bromide at 120 K

✍ Scribed by Bomfim, João A. S. ;Filgueiras, Carlos A. L. ;Howie, R. Alan ;Wardell, James L.

Publisher: International Union of Crystallography
Year: 2003
Tongue: English
Weight: 294 KB
Volume: 59
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536803002009

No coin nor oath required. For personal study only.

✦ Synopsis

ÁBr À is, to our knowledge, the ®rst reported example of a simple salt of cationic mono-Nprotonated 1,10-phenanthroline-5,6-dione. All of the atoms lie on a crystallographic mirror plane and the cation is therefore totally planar. As a consequence, the compound has a well de®ned layer structure in which NÐHÁ Á ÁBr, CÐHÁ Á ÁBr and CÐHÁ Á ÁO contacts within the layers interconnect the ionic species.

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We gratefully acknowledge the financial support of the Natural Science Foundation of China (No. 20573114).

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