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5,5a-Diallyl-5,5a,13,14-tetra­hydro-12H-di-1,3-benzimidazolo[1,2-a;1′,2′-c][1,4]diazepine

✍ Scribed by Yıldırım, Sema Öztürk ;Akkurt, Mehmet ;Yılmaz, Ülkü ;Küçükbay, Hasan ;McKee, Vickie

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
186 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 23 H 24 N 4 , was synthesized from 3,3 0diallyl-1,1 0 -propylenedi(benzimidazole) dibromide and NaH in tetrahydrofuran solution. In the molecule, the diazepine ring exhibits a boat conformation.

📜 SIMILAR VOLUMES

Syntheses of 7-phenyl-5h-thiazolo[5,4-e]
Syntheses of 7-phenyl-5h-thiazolo[5,4-e]pyrrolo[1,2-a][1,4]diazepin-10(9h)one,7-phenyl-5h-thiazolo[5,4-e][1,2,3,4]tetrazolo[5,1-c]-pyrrolo[1,2-a][1,4]diazepine and 7-phenyl-5h-thiazolo[5,4-e]-[1,3,4] triazolo [5,1-c]pyrrolo [1,2-a] [1,4] diazepines
✍ A. Shafiee; M. Shekarchi 📂 Article 📅 2002 🏛 Journal of Heterocyclic Chemistry 🌐 English ⚖ 48 KB 👁 1 views

## Abstract Fused tricyclic 7‐phenyl‐5__H__‐thizolo[5,4‐__e__]pyrrolo[1,2‐__a__][1,4]diazepin‐10(9__H__)one (**10**) was prepared by thermolysis of 2‐phenyl‐4‐(1‐pyrrolylmethyl)thiazole‐5‐carbonyl azide (**9**) in acetic acid. In addition, starting from **10**, 7‐phenyl‐5__H__‐thiazolo [5,4‐__e__][

Synthesis of [1,2-a] benzimidazolo-1,3,5
Synthesis of [1,2-a] benzimidazolo-1,3,5-triazin-2-thione, [1,2-a] benzimidazolo-1,3,5-thiadiazin-2-thione, [1,2-a] benzimidazolo-1,3,5-triazin-2-amine, and [1,2-a] benzimidazol-2-yl amidrazone
✍ A. Hajri; R. Abderrahim 📂 Article 📅 2010 🏛 John Wiley and Sons 🌐 English ⚖ 90 KB 👁 1 views

## Abstract __N__‐benzimidazol‐2‐yl imidate type **1** reacts with thiourea, carbon disulfide, cyanamide, and hydrazide to give, respectively, [1,2‐__a__] benzimidazolo‐1,3,5‐triazin‐2‐thione **2**, [1,2‐__a__] benzimidazolo‐1,3,5‐thiadiazin‐2‐thione **3**, [1,2‐__a__] benzimidazolo‐1,3,5‐triazin‐2