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5,5-Dimethyl-1,2-dithia-3,7-diselenacycloheptane—A Storable Source of Disulfur, S2

✍ Scribed by Prof. Dr. Max Schmidt; Dr. Udo Görl

Book ID
101557647
Publisher
John Wiley and Sons
Year
1987
Tongue
English
Weight
263 KB
Volume
26
Category
Article
ISSN
0044-8249

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7,7-Dimethyl-2-phenyl-6,7-dihydro-1,2,4-
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✍ Dolzhenko, Anton V. ;Tan, Geok Kheng ;Koh, Lip Lin ;Dolzhenko, Anna V. ;Chui, Wa 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 494 KB

The title compound, C 12 H 14 N 6 , was synthesized via cyclocondensation of 5-guanidino-3-phenyl-1,2,4-triazole with acetone. Only one tautomeric form with the NH H atom vicinal to the methyl groups was observed in the crystal structure. The triazine ring adopts a flattened half-boat conformation.

5,5-Dimethyl-2-phenyl-4,5-dihydro-1,2,4-
5,5-Dimethyl-2-phenyl-4,5-dihydro-1,2,4-triazolo[1,5-a][1,3,5]triazin-7-amine
✍ Dolzhenko, Anton V. ;Tan, Geok Kheng ;Koh, Lip Lin ;Dolzhenko, Anna V. ;Chui, Wa 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 945 KB

The title compound, C 12 H 14 N 6 , was synthesized via cyclocondensation of 5-amino-1-guanyl-3-phenyl-1,2,4-triazole with acetone. Only one tautomeric form with an H atom at the triazine N atom was observed in the crystal structure. The compound crystallizes with two almost identical molecules in t