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51 V Chemical Shielding and Quadrupole Coupling in Ortho- and Metavanadates from 51 V MAS NMR Spectroscopy

✍ Scribed by Skibsted, Jørgen; Jacobsen, Claus J. H.; Jakobsen, Hans J.

Book ID
126899775
Publisher
American Chemical Society
Year
1998
Tongue
English
Weight
174 KB
Volume
37
Category
Article
ISSN
0020-1669

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Quadruple coupling and chemical shift anisotropy are of comparable magnitudes in the NMR of quadrupole nuclei of heavy atoms. Magic angle spinning (MAS) and off-MAS NMR spectra of 'lV and 59C0 nuclei were measured for vanadium(V)aitrilotriacetate complex, cobalt(0) acetylacetonate and ammonium metav