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5-Methoxy-4-(4-methoxy­phenyl)­isochroman-3-ol

✍ Scribed by Palusiak, Marcin ;Małecka, Magdalena ;Rybarczyk-Pirek, Agnieszka ;Epsztajn, Jan ;Bieniek, Adam ;Kowalska, Justyna A.

Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
252 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title compound, C 17 H 18 O 4 , the hydroxyl and methoxyphenyl substituents are in axial positions. The heterocyclic ring adopts a half-chair conformation. The molecules are linked by OÐHÁ Á ÁO hydrogen bonds, leading to dimerization.

📜 SIMILAR VOLUMES

(3S,4R)-4-(2,5-Di­methoxy­phenyl)-8-meth
(3S,4R)-4-(2,5-Di­methoxy­phenyl)-8-methoxy­isochroman-3-ol
✍ Palusiak, Marcin ;Małecka, Magdalena ;Grabowski, Sławomir J. ;Epsztajn, Jan ;Bie 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 324 KB

In the title compound, C 18 H 20 O 5 , the hydroxyl and dimethoxyphenyl substituents are in axial positions. The heterocyclic ring is in a half-chair conformation. The molecules are linked by OÐHÁ Á ÁO hydrogen bonds, leading to the formation of a chain extended throughout the whole of the crystal.

8-Methoxy-4-(4-methoxyphenyl)isochroman-
8-Methoxy-4-(4-methoxyphenyl)isochroman-3-ol
✍ Palusiak, Marcin ;Grabowski, Sławomir J. ;Epsztajn, Jan ;Kowalska, Justyna A. 📂 Article 📅 2003 🏛 International Union of Crystallography 🌐 English ⚖ 237 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.006 A Ê R factor = 0.069 wR factor = 0.185 Data-to-parameter ratio = 7.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Methyl [5-methoxy-4-(3-methoxy­phenyl)­i
Methyl [5-methoxy-4-(3-methoxy­phenyl)­isochroman-3-yl]­acetate
✍ Palusiak, Marcin ;Małecka, Magdalena ;Grabowski, Sławomir J. ;Epsztajn, Jan ;Bie 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 218 KB

Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.004 A Ê R factor = 0.055 wR factor = 0.157 Data-to-parameter ratio = 13.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-(4-Methoxy­phenyl)but-3-yn-1-ol
1-(4-Methoxy­phenyl)but-3-yn-1-ol
✍ Bats, Jan W. ;Fischer, Dirk ;Hashmi, A. Stephen K. 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 424 KB

Molecules of the title compound, C 11 H 12 O 2 , are connected by intermolecular OÐHÁ Á ÁO hydrogen bonds to form helices running in the b direction. These helices are further stabilized by intermolecular CÐHÁ Á Á%(phenyl) interactions.