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5-indanyl acrylate monomer: Synthesis, characterization and copolymerization with glycidyl methacrylate

✍ Scribed by S. Balasubramanian; B.S.R. Reddy

Publisher
Elsevier Science
Year
1996
Tongue
English
Weight
416 KB
Volume
32
Category
Article
ISSN
0014-3057

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✦ Synopsis

Ahstrac-A

new monomer, S-indanyl acrylate (IdA), has been synthesized from the precursor viz., Sindanol, and characterized by FT-IR, 'H-NMR and "C-NMR spectroscopies. Homo-and copolymetization of IdA with glycidyl methacrylate (GMA) have been carried out in benzene by free radical polymerization at 70Β°C utilizing 2,2'-azobisisobutyronitrile (AIBN). Poly(IdA) and MAGMA copolymers were characterized by 'H-NMR and "C-NMR, and the copolymer compositions were evaluated by 'H-NMR spectroscopy. The reactivity ratios were estimated using Fineman-Ross, Kelen-Tudos and extended Kelen-Tudos methods. The Q and e values for IdA have been determined adopting the Alfrey-Price scheme. By TGA and DSC analyses, the thermal properties of the polymers have been studied.

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