5-(Furan-2-yl)-4-(p-tolyl)-2,4-dihydro-1,2,4-triazole-3-thione
✍ Scribed by Dege, Necmi ;Andac, Omer ;Cansız, Ahmet ;Çetin, Ahmet ;Şekerci, Memet ;Dinçer, Muharrem
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 287 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.005 A Ê R factor = 0.058 wR factor = 0.110 Data-to-parameter ratio = 15.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 296 K Mean '(C±C) = 0.003 A Ê R factor = 0.039 wR factor = 0.096 Data-to-parameter ratio = 17.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the molecule of the title compound, C 5 H 7 N 7 S, the essentially planar triazole ring and the 4-amino-5-mercapto-1,2,4-triazole moiety make a dihedral angle of 70.97 (5) . In the crystal structure, weak intermolecular N-HÁ Á ÁN and N-HÁ Á ÁS hydrogen bonds stabilize the packing.
In the title compound, C 15 H 19 N 5 OS, the morpholine ring adopts a chair conformation. The mean plane of the pyridine ring makes a dihedral angle of 35.16 (7) with the triazole ring plane.
The title compound, C 13 H 13 N 5 S, possesses crystallographically imposed mirror symmetry. In the crystal structure, the molecules interact through strong intermolecular N-HÁ Á ÁN hydrogen bonds to form ribbons running parallel to the a axis.