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5-Fluoro­uracil–di­methyl­form­amide (2/1)

✍ Scribed by Hulme, Ashley T. ;Tocher, Derek A.

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
487 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

A solvate of 5-¯uorouracil with dimethylformamide (DMF), 2C 4 H 3 FN 2 O 2 ÁC 3 H 7 NO, is reported. It crystallizes in the monoclinic space group P2 1 /n, with two molecules of 5-¯uorouracil and one molecule of DMF in the asymmetric unit. This solvate exhibits a sheet structure, with the DMF molecules present on both surfaces of the sheet and 5-¯uorouracil molecules within the sheath of DMF molecules.

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trans-Di­aqua­bis­{2-[3-(di­methyl­amino
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✍ Yan, Ze-Qun 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 208 KB

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.009 A Ê Disorder in solvent or counterion R factor = 0.074 wR factor = 0.200 Data-to-parameter ratio = 11.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.