𝔖 Bobbio Scriptorium
✦   LIBER   ✦

5-(Benzo­[1,3]­dioxol-5-yl)-7-(4-chloro­phenyl)-3-methyl-1-phenyl-1,6,7,8-tetra­hydro­pyrazolo­[3,4-b][1,4]­diazepine

✍ Scribed by Low, John Nicolson ;Cobo, Justo ;Nogueras, Manuel ;Sánchez, Adolfo ;Insuasty, Braulio ;Mosquera, Mónica


Publisher
International Union of Crystallography
Year
2002
Tongue
English
Weight
263 KB
Volume
59
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis


Single-crystal X-ray study T = 120 K Mean '(C±C) = 0.003 A Ê R factor = 0.056 wR factor = 0.150 Data-to-parameter ratio = 16.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.


📜 SIMILAR VOLUMES


4-(4-Fluoro­phen­yl)-3-methyl-6-oxo-1-ph
✍ Wang, Jing ;Zhu, Song-Lei 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 78 KB

The title compound, C 20 H 15 FN 4 O, was synthesized by the reaction of 5-amino-3-methyl-1-phenylpyrazole with ethyl 2cyano-3-(4-fluorophenyl)-1-acylate in glycol under microwave irradiation. The tetrahydropyridine ring adopts a distorted envelope conformation. The pyrazole ring forms a dihedral an