4,4-Dimethyl-2-(2-methyl-1-propenyl)-2,6-diphenyl-2,3,4,5-tetrahydropyrimidine
✍ Scribed by Jones, Peter G. ;Hopf, Henning ;Lautenbach, Holger W.
- Publisher
- International Union of Crystallography
- Year
- 2003
- Tongue
- English
- Weight
- 191 KB
- Volume
- 59
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 295 K Mean '(C±C) = 0.003 A Ê R factor = 0.043 wR factor = 0.119 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The reaction of cinnamoyl isothiocyanate and aniline gave a the title cyclized thiourea, C 13 H 16 N 2 S. There are two molecules in the asymmetric unit. The pyrimidine-2-thione moiety in each molecule is almost perpendicular to the phenyl group. The molecules are linked by two intermolecular NÐHÁ Á
Single-crystal X-ray study T = 293 K Mean (C±C) = 0.003 A Ê Disorder in main residue R factor = 0.043 wR factor = 0.134 Data-to-parameter ratio = 12.4 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.