4,10a-(Epidithio)-4,4a,10,10a-tetrahydro-1H-5-oxaanthracen-1-ones, tetracycles with a novel heterocyclic ring system
β Scribed by Sandra Kolly; Hansrudolf Meier; Grety Rihs; Tammo Winkler
- Book ID
- 102258702
- Publisher
- John Wiley and Sons
- Year
- 1988
- Tongue
- German
- Weight
- 388 KB
- Volume
- 71
- Category
- Article
- ISSN
- 0018-019X
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β¦ Synopsis
The 4,4',6,6'-tetrasubstituted 2,2'-alkylidene-bisphenols 1 reacted with sulfur monochloride to give 4, IOa-(epi-dithi0)-4,4a,lO, 1Oa-tetrahydro-lH-5-oxaanthracen-I-ones (3 and 4). The structures of the products were elucidated by a combination of X-ray crystal-structure analysis and 'Hand "C-NMR spectroscopy.
π SIMILAR VOLUMES
## Abstract The title novel fused tricyclic phosphoroheterocycle, C~19~H~20~N~3~O~2~PS, was synthesized in an excellent yield of 88.5% via the reacβ tion of 1β(2βbromoethyl)β2,3βdihydroβ3βpropylβ1,3,2βbenzodiazaphosphorinβ4(1__H__)βone 2βoxide with phenyl isothiocyanate, which contains the proximat